Luminescence Chem Kit from Edmund Scientific 1 of 3
Posted on September 22nd, 2006 in Hands On/Build This!, Labs/Experiments, Photos/Videoes, Science!, The Never Ending Story/Other FLB Events | Comments Off on Luminescence Chem Kit from Edmund Scientific 1 of 3
Here comes that review we
were talking about. This is part 1 of 3 reviews on products by Edmund
Scientific. You know why? (Because we got 3 kits…) This one was a luminescence
kit. Now, because of one chemical provided in the lab, we decided to trek to
the local high school to the AP Chemistry teacher there for use of his lab and
fume hood. I would have done it at my house, but…I don’t trust my own hood
because I installed it myself.
Turns out…we didn’t use
the hood. Oh well. We do caution you though, that the MDS information on the
liquid solvent (DMS) indicates it is an irritant and is readily absorbed by the skin.
We should have used gloves. I was just really careful. Don’t follow my example.
K?
We unpacked the kit, and
found that it was nicely packed, with very good chemical safeguards. Every
bottle had an MDS sheet attached, which was a real plus. The only thing I found
slightly annoying was the lack of NaOH and beakers. Then again, beakers…I hope
you have if you are going to be doing this type of thing. Deep bowls work too…just
don’t use them afterwards. 😉
Oddly enough, our kit did not come with NaOH so we had to find some
NaOH. Granted, this is not one for the non-chemistry initiated. So, be ready to
follow directions on how to get a specific molar concentration NaOH. And
remember, when it tells you to only poor a few ml of the solution in, follow the directions.
We proceeded with safety
glasses, as it was fairly high concentration NaOH. Our first trial failed quite
miserably, owing to contamination in our beakers as well as a poor
concentration of NaOH. It turned out to be a sickly pale green color. We shook
it vigorously, used magnetic stirring rod on max, and it didn’t work.
Note that the sample on the right is the failed one. The one of the left was our final result
We did it again, with the
clean beaker and was very careful with NaOH, and low and behold, let there be light! We followed
directions and got a fairly bright liquid that glowed bright blue green. Increasing
the concentration of luminol did not affect the brightness, which was an
interesting sidetrack, although after we were through ogling the bright blue
light, we realized it was simply an inherent rate of the reaction. In common
language: ya aint goin to change it.
This was an interesting
kit, very straightforward, and fun. Slightly hard to comprehend chemically for
students, but hey, we’ve taken college chemistry, and it makes sense. This
product was quite nice, and the chemistry teacher was interested in it. You can
check out the home page here and the product page here. We are testing two
other products, which can be found here and here. Good stuff 😀